SKU: HI933-02
For scientists and professionals who need exact water content determination from 0.01 to 100%, our new generation of the Volumetric Karl Fischer Titrator is engineered to meet or exceed your technical requirements while delivering a lower cost of ownership. With cutting-edge features packed into a compact design, this titrator delivers accurate results and requires less space in the lab. Get accurate water content determination at the push of a button. Designed for the modern lab, this karl fischer titrator is the perfect fit for your testing environment.
SKU | HI933-02 |
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Product Name | Volumetric Karl Fischer Titrator – HI933 |
Quote Required | Yes |
Titration Range | 100 ppm to 100% |
Titration Resolution | 1 ppm to 0.0001% |
Measurement Units | %, ppm, mg/g, μg/g, mg, μg, mg/mL, μg/mL, mg/pc, μg/pc |
Sample Type | liquid or solid |
Pre-Titration Conditioning | automatic |
Background Drift Correction | automatic or user-selectable value |
Endpoint Criteria | fixed mV persistence, relative drift stop or absolute drift stop |
Dosing Type | dynamic with optional pre-dispensing |
Result Statistics | mean, standard deviation |
Dosing Accuracy | ±0.1% of full burette volume |
Syringe | 5 mL precision ground glass with PTFE plunger |
Valve | motor-driven 3-way, PTFE liquid contact material |
Tubing | PTFE with light block and thermal jacketing |
Dispensing Tip | glass, fixed position, anti-diffusing |
Titration Vessel | conical with operation volume between 50 and 150 mL |
Solvent Handling System | sealed system, integrated diaphragm air pump |
Connection Type | BNC |
Polarization Current | 1, 2, 5, 10, 15, 20, 30 or 40 uA |
mV Range | 2 mV to 1000 mV |
mV Resolution | 0.1 mV |
mV Accuracy | ±0.1% |
Burette | 5 mL burette |
Dosing Pump Resolution | 1/40000 of the burette volume (0.125 μL per dose) with 5 mL burette |
Stirrer Type | magnetic, optically regulated, digital stirre |
Stirrer Speed | 200 – 2000 RPM |
Stirrer Resolution | 100 RPM |
Titrator Methods | up to 100 standard and user defined |
Reports | up to 100 complete titration reports and drift rate reports |
Connectivity | USB |
Built-in Magentic Stirrer | magnetic, optically regulated, digital stirrer; 200 to 2000 rpm; resolution 100 rpm |
Display | 5.7” graphical color display with backlight |
Keypad | polyester |
Languages | English, Portuguese, Spanish, and French |
Power Supply | 100-240 Vac, 50/60 Hz / 0.5 Amps |
Environment | Operating |
Dimensions | 315 x 205 x 375 mm (12.4 x 8.1 x 14.8″) |
Weight | Approximate 4.3 kg (9.5 lbs) with 1 pump, stirrer and sensors |
Ordering Information | HI933 is supplied with HI76320 dual platinum pin electrode, dosing pump, 5 mL burette assembly with tubing, air pump/stirrer assembly with tubing, beaker and bottle top assemblies and all fittings, desiccant cartridges (4) with indicator desiccant, stir bar, waste bottle, calibration key, USB cable, power cable, USB flash drive, quality certificate, ISO 8655 burette compliance report, and instruction manual binder |
The dynamic titration speed allows for timely and accurate titration results by relating the amount of iodine generated to the mV response from the Karl Fischer reaction. This provides for a larger generation of iodine near the beginning of a titration and more precise pulses near the titration endpoint.
The HI934 automatically adjusts the titration calculation to account for the effects of any ambient humidity entering the titration cell. This provides a more accurate result by correcting for water not present in the actual sample.
The HI934 employs a dual platinum pin electrode for bivoltammetric endpoint determination. Users may choose termination criteria based on mV stability times or drift rates.
A pre-titration stage eliminates residual water present in the solvent and the cell, providing a reliable baseline start to analysis. Standby mode then keeps the solvent dry between titrations and when the titrator is not in use.
Two styles of generators are available for the HI934; a fritted design ideal for samples with low water content and high accuracy demand; and a fritless generator allowing for easier cleaning and maintenance.
Our dosing algorithm allows for an extremely small amount of iodine necessary for the Karl Fischer reaction to be generated electrolytically using a pulsed current up to 400 mA, delivering iodine accurately and precisely.
The glass titration cell and PTFE tubing is designed to withstand the harsh solvents and reagents involved in Karl Fischer reactions.
Ground glass joints completely seal the glass titration cell, minimizing exposure to ambient humidity, keeping the system dry, and reducing reagent consumption while saving time between titrations. Solvent may be exchanged in a matter of seconds with a quick fitting adjustment.
High efficiency molecular sieve desiccant helps maintain low and stable drift rates within the titration cell while preventing the ingress of ambient humidity into the sealed solvent system.
A large, color LCD screen clearly shows the chosen titration method along with results, units, total water, drift rate, and mV value.
A real-time titration curve can be displayed during each titration; this feature is useful when new methods are tested or when a procedure requires optimization.
Virtual key selections present on the display allow for simple and quick navigation between screens and menus without getting lost in a nest of information.
Each titration report is fully customizable so users can ensure they are storing and filing the appropriate data required for their application and procedures.
All necessary GLP (Good Laboratory Practice) information can be recorded with each sample including: sample identification, company and operator name, date, time, and electrode ID codes.
Data can easily be transferred to a USB flash drive or PC with the Hanna HI900PC application software. The USB port allows for the transfer of titration methods, titration reports, and software upgrades via USB flash drive.
Sample size may be automatically entered from any laboratory analytical balance with a RS232 serial output saving time and labor.
Users can print reports directly from the titrator using a standard parallel printer. An external monitor and keyboard may be attached for added versatility, as well as an analytical balance for automatic sample mass entry for titrations.
The HI934 can store up to 100 user-defined or standard titration methods. Each method may be customized and optimized for performance based on application and user requirements.
Onsite installation, training, and customization is available from one of our Applications or Service experts. Hanna offers continued support via phone or webinar for any questions you might have along the way.
Our technical experts can program and customize standard methods developed by such affiliations as ISO, ASTM, AOAC, AOCS, EPA, and more directly onto your titrator. Ask our Sales Consultants which standard methods are possible with our HI934 Karl Fischer system.
Measurement | ||||
Range | 1 ppm to 5% | |||
Resolution | 0.1 ppm | |||
Result Units | % ppm, mg/g, µg/g, mg, µg, mg/mL, µg/mL, mgBr/100g, gBr/100g, mgBr, gBr | |||
Sample type | liquid or solid (external dissolution or extraction) | |||
Determination | ||||
Pre Titration conditioning | automatic | |||
Background Drift Correction | automatic or user selectable value | |||
Endpoint Criteria | fixed mV persistence, relative drift stop, or absolute drift stop | |||
Dosing | Dynamic with 3 speed settings | |||
Result Statistic | mean, standard deviation | |||
Titration Vessel | ||||
Type | borosilicate glass with standard taper glass joint connections | |||
Operating volume | 100 to 200 mL | |||
Septum | silicone rubber | |||
Septum Cap Thread | GL-18 | |||
Reagent Port | Standard Taper 19 | |||
Detector Electrode | ||||
Type/Connection | Dual platinum pin, polarisation electrode/BNC Connector | |||
Glass connection | standard Taper 14/20 | |||
Polarisation Current | 1, 2, 5, or 10 µA | |||
Voltage Range | 2 to 1100mV | |||
Voltage Resolution 0.1mV | ||||
Accuracy (@25°C) | ±0.1% | |||
Generator Electrode | ||||
Type | diaphragm or diaphragm-less | |||
Electrode Type Detection | Automatic | |||
Electrical Connection | 5-pin connector with detachable cable | |||
Glass Connection | standard taper 29/12 | |||
Maximum Current | 400 mA | |||
Current Control | automatic or fixed (400 mA) | |||
Stirrer | ||||
Type | Magnetic, electronic regulated, digital stirrer | |||
Speed | 200 to 2000 RPM | |||
Resolution | 100 RPM | |||
External Stirrer | 4-pin mini DIN connection allows for the control of an external stirring apparatus | |||
Reagent Handling System | ||||
Type | sealed system with integrated diaphragm air pump | |||
Desiccant Type | Molecular sieves | |||
Bottle thread type | GL-45 | |||
Glass connection | standard taper 19 (using supplied adapter) | |||
Reagent/Waste Tubing | PTFE | |||
Additional Specifications | ||||
Display | 5.7” graphical colour display with backlight | |||
Peripheral Devices | PC (USB standard B), flash drive (USB standard A), analytical balance (DB-9 socket), printer (DB-25 socket), keyboard (6-pin mini DIN) | |||
Languages | English, Portuguese, Spanish and French | |||
Power supply/power draw | 100-240 VAC, 50/60 Hz/0.5 Amps | |||
Enclosure material | ABS/PC and stainless steel | |||
Keypad | polyester | |||
Operating Environment | 10 to 40°C; up to 80% RH | |||
Storage environment | -20 to 70°C; up to 95% RH | |||
Dimensions | 315 x 205 x 375 mm | |||
Weight | approx. 4.3kg with 1 pump, stirrer and sensors | |||
Ordering information | HI-934D-01 and HI-934D-02 are supplied with diaphragm HI-934-01 and HI-934-02 are supplied without diaphragm All models include: Dual platinum pin electrode, air pump/stirrer assembly, titration vessel assembly (glass vessel, accessory port stopper, sample port cap and septum, stir bar, desiccant, desiccant cartridge fittings), vessel support with adapter, pump locking screw with plastic head, reagent bottle assembly (bottle cap, desiccant, desiccant cartridge, fittings, tubing – silicone and PTFE), water bottle assembly (waste bottle, bottle cap, desiccant, desiccant cartridge, fittings, tubing – silicone and PTFE), calibration key, reagent exchange adapter, accessory holder assembly, joint grease, Karl Fischer generator electrode (removable generator electrode cable), USB cable, USB storage device, HI-900 PC application software, power adapter, quality certificate and instruction manual binder. |